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Oxidative Addition of Isocyanide Dichlorides to Metal Complexes

✍ Scribed by Dr. Wolf Peter Fehlhammer; Andreas Mayr; Bernhard Olgemöller

Publisher
John Wiley and Sons
Year
1975
Tongue
English
Weight
221 KB
Volume
14
Category
Article
ISSN
0044-8249

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from a benzene solution at room temperature. 1 H NMR (400.1 MHz, C 6 D 6 ): d = 2.71À2.60 (m, 6 H, Cy), 2.23À2.15 (m, 12 H, Cy), 1.81À1.20 (m, 48 H, Cy); 11 B{ 1 H} NMR (128.4 MHz, C 6 D 6 ): d = 30 ppm; 13 C{ 1 H} NMR (100.6 MHz, C 6 D 6 ): d = 35.8 (vt, N =j 1 J P-C + 3 J P-C j= 28 Hz, C 1 Cy), 30