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Optosensing properties of fac-Re(CO)3(dpknph)Cl (dpknph=di-2-pyridyl ketone p-nitrophenyl hydrazone)

✍ Scribed by Mohammed Bakir; Kamaluddin Abdur-Rashid; Willem H. Mulder

Book ID: 117225189
Publisher: Elsevier Science
Year: 2000
Tongue: English
Weight: 157 KB
Volume: 51
Category: Article
ISSN: 0039-9140
DOI: 10.1016/s0039-9140(99)00322-7

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The reaction between di-2-pyridyl ketone 4-aminobenzoylhydrazone hydrate (dpk4abh.H 2 O) and [Re(CO) 5 Cl] in refluxing toluene gave fac-[Re(CO) 3 (j 2 -N,N-dpk4abh)Cl]. Hydrolysis of fac-[Re(CO) 3 (j 2 -N,N-dpk4abh)Cl] to form fac-[Re(CO) 3 (j 3 -N,O,N-dpkO,OH)] occurs in wet solvents. The identity