One-Pot Synthesis of [(C 6 F 5 ) 2 BH 2 ] − from C 6 F 5 MgBr/BH 3 ·SMe 2 and Its in Situ Transformation to Piers’ Borane
✍ Scribed by Schnurr, Anna; Samigullin, Kamil; Breunig, Jens M.; Bolte, Michael; Lerner, Hans-Wolfram; Wagner, Matthias
- Book ID
- 127307892
- Publisher
- American Chemical Society
- Year
- 2011
- Tongue
- English
- Weight
- 898 KB
- Volume
- 30
- Category
- Article
- ISSN
- 0276-7333
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## Abstract A convenient method of preparing 2‐octyl (4‐amino‐3,5‐dichloro‐6‐fluoro‐2‐pyridinyloxy‐2,6‐^14^C)acetate from glutarimide‐2,6‐^14^C is described. The process includes a novel one‐step conversion of glutarimide‐2,6‐^14^C to pentachloropyridine‐2,6‐^14^C.