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One-pot synthesis of benzothiazolines and napthathiazolines via cascade ortho-lithiation, cyclisation and elimination of N-arylsulfonyl lactams

✍ Scribed by Harling, John. D.; Steel, Patrick. G.; Woods, Tom. M.; Yufit, Dmitry S.

Book ID
119942262
Publisher
Royal Society of Chemistry
Year
2007
Tongue
English
Weight
166 KB
Volume
5
Category
Article
ISSN
1477-0520

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ChemInform Abstract: One-Pot Synthesis o
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✍ John D. Harling; Patrick G. Steel; Tom. M. Woods; Dmitry S. Yufit πŸ“‚ Article πŸ“… 2008 πŸ› John Wiley and Sons βš– 49 KB πŸ‘ 1 views

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ChemInform Abstract: One-Pot Synthesis of Substituted Isoindolin-1-ones via Lithiation and Substitution of Nβ€²-Benzyl-N,N-dimethylureas.
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## Abstract Lithiation of ureas (I) and (VI) followed by quenching with various electrophiles, such as aldehydes (II), ketones (IV) and alkyl halides (VII) affords the corresponding 3‐substituted isoindolin‐1‐ones (III), (V), and (VIII), respectively, in good yields.