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One-Pot synthesis of a novel compound N-hydroxydecahydroacridine under microwave irradiation

✍ Scribed by Shujiang Tu; Fang Fang; Songlei Zhu; Tuanjie Li; Xiaojing Zhang; Qiya Zhuang

Publisher
Journal of Heterocyclic Chemistry
Year
2004
Tongue
English
Weight
173 KB
Volume
41
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

A novel reaction to synthesis a series new N‐hydroxyldecahydroacridine derivatives by a one‐pot condensation of aldehyde, 1,3‐dicarbonyl compound and NH~2~OH in glycol under microwave irradiation is described. N‐hydroxyldecahydroacridine was obtained in excellent yields (81–95%) within short reaction time (4–7 min)

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✍ Shujiang Tu; Xiaojing Zhang; Feng Shi; Tuanjie Li; Qian Wang; Xiaotong Zhu; Jinp πŸ“‚ Article πŸ“… 2005 πŸ› Journal of Heterocyclic Chemistry 🌐 English βš– 104 KB πŸ‘ 1 views

A series of new N-cyclopropyldecahydroacridine-1,8-dione derivatives were synthesized by one-pot reaction of aromatic aldehyde, dimedone (or 1,3-cyclohexanedione) and cyclopropanamine in solution of glycol and water under microwave irradiation with excellent yields (78-94%) and short reaction time (