## Combined utilization of 'H-IH homonuclear and 'H-l'C heteronuclear N M R chemical shift correlations, two-dimensional J-resolved 'H NMR measurements and homonuclear 'H double resonance experiments allowed specific assignments for both 'H and -C NMR frequencies to be made for the tricyclic sesqu
One- and two-dimensional NMR studies of plasmalogens (alk- l -enyl-phosphatidylethanolamine)
✍ Scribed by R. Sacchi; I. Medina; L. Paolillo
- Publisher
- Elsevier Science
- Year
- 1995
- Tongue
- English
- Weight
- 477 KB
- Volume
- 76
- Category
- Article
- ISSN
- 0009-3084
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✦ Synopsis
~H and ~3C nuclear magnetic resonance (NMR) spectra of phosphatidylethanolamine plasmalogen were studied. Resonances in both spectra were assigned by conventional one-and two-dimensional NMR techniques. Distinctive signals corresponding to the olefinic carbons near the vinyl ether group were shown to be the most useful in both qualitative and quantitative analysis, The plasmalogen content in different fish lipid samples, as determined by ~3C-NMR spectro'scopy, was in good agreement with the data obtained by gas chromatograpy.
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