𝔖 Bobbio Scriptorium
✦   LIBER   ✦

On the Synthesis and Characterization of N-Formyl Glutathione and N-Acetyl Glutathione

✍ Scribed by E.J. Levy; M.E. Anderson; A. Meister

Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
243 KB
Volume
214
Category
Article
ISSN
0003-2697

No coin nor oath required. For personal study only.

✦ Synopsis

Treatment of glutathione (GSH) with formic acid and acetic anhydride leads to preparation of crystalline (N) formyl GSH. This is the first characterized preparation of (N)-formyl GSH; this product was previously erroneously thought to be (N)-acetyl GSH. Authentic (N)-acetyl GSH (crystalline) was prepared by treating GSH with acetic acid and acetic anhydride. The (N)-acylated derivatives were characterized by ({ }^{1} H) NMR and mass spectroscopy. c 1993 Academic Press, Inc.

πŸ“œ SIMILAR VOLUMES

Synthesis and Characterization of the Se
Synthesis and Characterization of the Selenium Analog of Glutathione Disulfide
✍ T. Tamura; T. Oikawa; A. Ohtaka; N. Fujii; N. Esaki; K. Soda πŸ“‚ Article πŸ“… 1993 πŸ› Elsevier Science 🌐 English βš– 290 KB

We synthesized the selenium analog of glutathione disulfide by a liquid phase method and named it glutaselenone (i.e., gamma-L-glutamyl-L-selenocysteinylglycine) diselenide. The selenol of selenocysteine was protected by the p-methoxybenzyl group, which was removed by acidolysis with trifluoroacetic

Synthesis, characterization and fluoresc
Synthesis, characterization and fluorescent properties of cerium(III) glutathione complex
✍ Guo-Cheng Han; You-Nian Liu πŸ“‚ Article πŸ“… 2009 πŸ› John Wiley and Sons 🌐 English βš– 465 KB πŸ‘ 1 views

## Abstract The cerium (III) glutathione complex was synthesized by the redox reaction of cerium (IV) with glutathione reduced (GSH) in aqueous solution. The Job‐plots indicate an ML (L = GSSG) stoichiometry of the complex. The fluorescent properties of the compound were investigated. The as‐prepar

Quantitative determination of the glutat
Quantitative determination of the glutathione, cysteine, and N-acetyl cysteine conjugates of acetaminophen by high-pressure liquid chromatography
✍ A.R. Buckpitt; D.E. Rollins; S.D. Nelson; R.B. Franklin; J.R. Mitchell πŸ“‚ Article πŸ“… 1977 πŸ› Elsevier Science 🌐 English βš– 604 KB

A quantitative method for the estimation of the glutathione, cysteine, and N-acetyl cysteine conjugates of acetaminophen obtained from microsomal incubations has been developed using high-pressure liquid chromatography (HPLC). As little as 5 ng of the thiol conjugates of [ring-Tlacetaminophen can be