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On the structure of a proposed mixed-valent analogue of the diiron subsite of [FeFe]-hydrogenase

✍ Scribed by Best, Stephen P.; Borg, Stacey J.; White, Jonathan M.; Razavet, Mathieu; Pickett, Christopher J.

Book ID
111687583
Publisher
Royal Society of Chemistry
Year
2007
Tongue
English
Weight
494 KB
Volume
42
Category
Article
ISSN
1359-7345

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31 P NMR (202 MHz, CD 2 Cl 2 ): d = 74.1, 25.0 ppm. IR (CH 2 Cl 2 ): n ˜CO = 2002, 1955 cm Γ€1 ; n ˜NO = 1772 cm Γ€1 . ESI-MS: m/z 762.2 ([Fe 2 -(S 2 C 2 H 4 )(CO) 2 (NO)(PMe 3 )(dppv)] + ). Elemental analysis calcd