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On the perchlorination of 2-hydroxybiphenyl and 2-(2,4-dichlorophenoxy)-4,5,6-trichlorophenol and their methyl ethers

✍ Scribed by Anders Garå; Carl-Axel Nilsson; Kurt Andersson


Book ID
119020776
Publisher
Elsevier Science
Year
1980
Tongue
English
Weight
264 KB
Volume
9
Category
Article
ISSN
0045-6535

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Synthesis of [4″-3H]- and [4,4,5,5-2H4]-
✍ Gerd Kloster; Johannes Odenthal 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 205 KB 👁 1 views

## Abstract [4″‐^3^H]‐2‐(1‐[2″,6″‐Dichlorophenoxy]‐ethyl‐Δ^2^‐imidazoline) was prepared from [4‐^3^H]‐2,6‐dichlorophenol in two different ways. By reaction of 2,6‐dichlorophenol with 2‐(α‐chloroethyl)‐Δ^2^‐imidazoline, the radiochemical yield, at a specific activity of 173.9 mCi/mmole, was 12.8 %.