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On-line hydrogenation of fatty acid methyl esters in capillary gas chromatography

✍ Scribed by Kuzmenko, T. E. ;Samusenko, A. L. ;Uralets, V. P. ;Golovnya, R. V.

Publisher
John Wiley and Sons
Year
1979
Tongue
English
Weight
164 KB
Volume
2
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

An injection splitter in front of a glass capillary column was used for the hydrogenation of fatty acid methyl esters (FAME) mixtures. Hydrogenation followed by gas chromatographic analysis on capillary columns permitted detection and identification in complicated natural mixtures of branched fatty acids, showing minor structural differences, in quantities down to 10^βˆ’8^g.

The technique described, apart from its suitability for FAME analysis, shows promise for structure determination studies of other classes of compounds.

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