Proton transfer chemical ionization mass spectrometry of fatty acid methyl esters separated by gas chromatography: quantitative aspects
β Scribed by Eric D. Dodds; Mark R. McCoy; Lorrie D. Rea; John M. Kennish
- Publisher
- John Wiley and Sons
- Year
- 2005
- Tongue
- English
- Weight
- 82 KB
- Volume
- 107
- Category
- Article
- ISSN
- 1438-7697
No coin nor oath required. For personal study only.
π SIMILAR VOLUMES
Trimethylsilylated methyl esters of octadecadienoic, eicosadienoic, and octadecatrienoic acids, after stereospecific oxidation, were investigated by combined gas chromatography-chemical ionization mass spectrometry. Molecular weight could be determined by the ions at m/e(M -1)' and (M + 73)+ and the
## Abstract This paper reports the development of a technique for identifying and confirming chlorinated fatty acids previously detected in fish by gas chromatography (GC) with halogenβspecific detection (XSD). Fatty acid methyl esters (FAMEs) including chlorinated FAMEs within fractions of reverse
An analytical method for the separation and quantitation of acyl-CoA thioesters by gas chromatography-mass spectrometry is described. The method utilizes glycine aminolysis of the acyl-CoA thiolesters, esterification with pentafluorobenzyl bromide followed by gas chromatographic separation, and dete