Nuclear overhauser effect in undecoupled NMR spectra of carbon-13
β Scribed by Ray Freeman; H.D.W Hill
- Publisher
- Elsevier Science
- Year
- 1971
- Weight
- 170 KB
- Volume
- 5
- Category
- Article
- ISSN
- 0022-2364
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π SIMILAR VOLUMES
Overlapping resonances in the two-dimensional nuclear Overhauser (NOESY) spectrum of the O-antigenic polysaccharide from Escherichia coli O147 have been resolved by recording a tilted projection of a threedimensional NOESY-HSQC spectrum, where the carbon-13 and proton evolutions are linked together.
## Abstract The feasibility of the application of selective ^13^Cο£Ώ{^1^H} nuclear Overhauser effect (NOE) measurements to organic structural analysis in ^13^C NMR spectroscopy has been investigated at 25 MHz using citraconic anhydride and the methyl ester of pentalenolactone as model compounds. This
Various algorithms for solving the Solomon equations describing nuclear Overhauser effects (noes) in NMR spectroscopy have been compared. The applicability of the eigenvalue/eigenvector and the numerical integration approaches have been investigated. The eigenvalue/eigenvector approach is not a comp