The product is formed quantitatively if the reactants (on a 2-molar scale, slight excess of SF4) are heated a t 50°C in a closed vessel (200 ml) for 2 hr. The trimethylfluorosilane and the excess of sulfur tetrafluoride can be separated by lowtemperature vacuum-distillation, the pure product (1) rem
N,N′-Dihalogen-S,S-dimethylschwefeldiimid
✍ Scribed by R. Appel; Prof. Dr. D. Hänssgen
- Publisher
- John Wiley and Sons
- Year
- 1967
- Tongue
- English
- Weight
- 106 KB
- Volume
- 79
- Category
- Article
- ISSN
- 0044-8249
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