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NMR structure analysis of uniformly13C-labeled carbohydrates

✍ Scribed by Fontana, Carolina; Kovacs, Helena; Widmalm, Göran

Book ID
125362857
Publisher
Springer Netherlands
Year
2014
Tongue
English
Weight
974 KB
Volume
59
Category
Article
ISSN
0925-2738

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📜 SIMILAR VOLUMES

13C NMR analysis of specifically labeled
13C NMR analysis of specifically labeled [13C] azobenzenes
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## Abstract ^13^C NMR chemical shifts and ^13^C^13^C couplings for six specifically labeled [^13^C] azobenzenes are reported. Coupling magnitudes depend on the position of labeling and the nature of the substituents.

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The REDOR and CPMAS techniques are applied for measuring 13C-15N dipolar coupling constants in glycine. It is shown that the selective CP or SPECIFIC CP technique removes the coherent evolution of the spin system under homonuclear 13C-13C J couplings. While the large coupling constant (approximately