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Nitrogen-15 labeled deoxynucleosides. Synthesis of 15N6-and 15N1-deoxyadenosines from deoxyadenosine

✍ Scribed by Gao, X.; Jones, R. A.

Book ID: 111657482
Publisher: American Chemical Society
Year: 1987
Tongue: English
Weight: 389 KB
Volume: 109
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00238a063

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## Abstract The synthesis of ^15^N‐labelled nornicotine **2** and ^15^N‐labelled nicotine **1** is described via the reductive aminocyclization of a 1,4‐ketoaldehyde with a corresponding amine in the presence of sodium cyanoborohydride. Yields of 30% and 26%, respectively, were obtained from 3‐brom