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Nitrogen-15-labeled deoxynucleosides. 4. Synthesis of [1-15N] and [2-15N]-labeled 2'-deoxyguanosines

✍ Scribed by Goswami, Bhaswati; Jones, Roger A.

Book ID: 126903022
Publisher: American Chemical Society
Year: 1991
Tongue: English
Weight: 488 KB
Volume: 113
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00002a037

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## Abstract The synthesis of ^15^N‐labelled nornicotine **2** and ^15^N‐labelled nicotine **1** is described via the reductive aminocyclization of a 1,4‐ketoaldehyde with a corresponding amine in the presence of sodium cyanoborohydride. Yields of 30% and 26%, respectively, were obtained from 3‐brom