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Nickel-Catalyzed Borylation of Aryl Halides with 4,4,6-Trimethyl-1,3,2-dioxaborinane

✍ Scribed by Murata, Miki; Sogabe, Yosuke; Namikoshi, Takeshi; Watanabe, Shinji

Book ID: 118255612
Publisher: Japan Institute of Heterocyclic Chemistry
Year: 2012
Tongue: English
Weight: 638 KB
Volume: 86
Category: Article
ISSN: 0385-5414
DOI: 10.3987/com-12-s(n)28

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## Abstract We describe a convenient preparation of 4,6,6‐trimethyl‐1,3,2‐dioxaborinane (MethylPentaneDiolBorane, MPBH) and demonstrate that it is an excellent reagent for the [PdCl~2~(PPh~3~)~2~]‐catalyzed borylation of aryl bromides and iodides. The corresponding boronic esters undergo rapid Suzu