𝔖 Bobbio Scriptorium
✦   LIBER   ✦

New synthesis of 6-substituted benzo[a]pyrenes

✍ Scribed by Newman, Melvin S.; Lee, Len-Fang

Book ID
121016537
Publisher
American Chemical Society
Year
1975
Tongue
English
Weight
433 KB
Volume
40
Category
Article
ISSN
0022-3263

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Synthesis of carbon-13 labelled 6-substi
Synthesis of carbon-13 labelled 6-substituted benzo (a) pyrenes
✍ Robert E. Royer; Guido H. Daub; David L. Vander Jagt 📂 Article 📅 1976 🏛 John Wiley and Sons 🌐 French ⚖ 170 KB

## Abstract Sodium formate‐^13^C, prepared by hydrolysis of isopropyl formate, was allowed to react with N‐methylaniline hydrochloride to prepare the formylating agent N‐methylformanilide‐1‐^13^C. Formylation of benzo(a)pyrene with N‐methylformanilide‐1‐^13^C gave the 6‐^13^CHO derivative which was

Synthesis of 6-substituted benzo[a]pyren
Synthesis of 6-substituted benzo[a]pyrene-α-14C derivatives
✍ James L. Hicks; J. Richard Heys 📂 Article 📅 1981 🏛 John Wiley and Sons 🌐 French ⚖ 332 KB

## Abstract 6‐Lithiobenzo[__a__]pyrene was carbonated to produce benzo[__a__]pyrene‐6‐carboxylic‐^14^C acid, which was in turn used in the preparation of several derivatives. Methylation to the ester was followed by LiAlH~4~ reduction to 6‐hydroxymethyl‐^14^C‐benzo[__a__]pyrene. An efficient oxidat