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New synthesis of 6-substituted benzo[a]pyrenes involving 5a,6-epoxy-5a,6-dihydrobenzo[a]pyrene

✍ Scribed by Newman, Melvin S.; Lee, Len-Fang

Book ID: 126814913
Publisher: American Chemical Society
Year: 1974
Tongue: English
Weight: 129 KB
Volume: 39
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00926a035

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## Abstract Sodium formate‐^13^C, prepared by hydrolysis of isopropyl formate, was allowed to react with N‐methylaniline hydrochloride to prepare the formylating agent N‐methylformanilide‐1‐^13^C. Formylation of benzo(a)pyrene with N‐methylformanilide‐1‐^13^C gave the 6‐^13^CHO derivative which was