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New method of tris(trimethylsilyl) antimonite preparation

✍ Scribed by S. V. Basenko; M. G. Voronkov; Cao Meihua; I. A. Gebel’

Book ID
111459780
Publisher
Springer
Year
2008
Tongue
English
Weight
125 KB
Volume
78
Category
Article
ISSN
1070-3632

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A new preparation of trimethylsilyl ethe
A new preparation of trimethylsilyl ethers
✍ Harold W. Pinnick; Bolkrishna S. Bal; Nordin H. Lajis 📂 Article 📅 1978 🏛 Elsevier Science 🌐 French ⚖ 106 KB

We wish to report a new method for the prepamtion of trimethylsilyl (TMS) ethers frcm alcohols under mildly acidic conditions. This compliments the most common procedure for the prepamtion of this popular protecting group which uses TA4.S chloride and a base like triethylamine. ## 2,3 Our approac