𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Natural-Abundance 43 Ca Solid-State NMR Spectroscopy of Bone

✍ Scribed by Xu, Jiadi; Zhu, Peizhi; Gan, Zhehong; Sahar, Nadder; Tecklenburg, Mary; Morris, Michael D.; Kohn, David H.; Ramamoorthy, Ayyalusamy

Book ID
126941248
Publisher
American Chemical Society
Year
2010
Tongue
English
Weight
1009 KB
Volume
132
Category
Article
ISSN
0002-7863

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Natural abundance high-resolution solid
Natural abundance high-resolution solid state 2H NMR spectroscopy
✍ Abil E. Aliev; Kenneth D.M. Harris; David C. Apperley 📂 Article 📅 1994 🏛 Elsevier Science 🌐 English ⚖ 519 KB

We report for the first time an approach for natural abundance solid state \*H NMR spectroscopy involving magic angle sample spinning (MAS), high-power 'H decoupling (HPPD) and 'H-'H cross polarization (CP). Taking tetrakis (trimethylsilyl)silane (TTMSS), adamantane, I-chloroadamantane, hexamethylbe

Natural abundance 43Ca solid-state NMR c
Natural abundance 43Ca solid-state NMR characterisation of hydroxyapatite: identification of the two calcium sites
✍ Danielle Laurencin; Alan Wong; Ray Dupree; Mark E. Smith 📂 Article 📅 2008 🏛 John Wiley and Sons 🌐 English ⚖ 171 KB

## Abstract Natural abundance ^43^Ca solid‐state NMR of hydroxyapatite (Ca~10~(PO~4~)~6~(OH)~2~) was performed at three different fields (8.45, 14.1 and 18.8 T). The two crystallographically distinct calcium sites of the apatite structure were spectroscopically resolved at 18.8 T. The ^43^Ca NMR in

Proton-Detected Solid-State NMR Spectros
Proton-Detected Solid-State NMR Spectroscopy of Natural-Abundance Peptide and Protein Pharmaceuticals
✍ Donghua H. Zhou; Gautam Shah; Charles Mullen; Dennis Sandoz; Chad M. Rienstra 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 581 KB

## Abstract **The natural way**: A sensitive NMR spectroscopic method is developed to obtain well‐resolved two‐dimensional spectra (^15^N–^1^H and ^13^C–^1^H) for natural‐abundance (that is, without the need for isotopic enrichment) large‐molecule samples, such as biopharmaceuticals. This method gi