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N-(6-Meth­oxy-2-methyl-8-quinol­yl)-4-n-propyl­benzene­sulfonamide

✍ Scribed by da Silva, Luiz Everson ;Joussef, Antonio Carlos ;Foro, Sabine ;Schmidt, Boris

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
313 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 299 K Mean (C-C) = 0.004 A R factor = 0.046 wR factor = 0.131 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

4-n-Propyl-N-(8-quinol­yl)benzene­sulfon
4-n-Propyl-N-(8-quinol­yl)benzene­sulfonamide
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In the title compound, C 18 H 18 N 2 O 2 S, the torsion angle about the N-S bond between the quinoline ring system and the benzene ring is À60.9 (2) . The NH group forms an intramolecular hydrogen bond to the quinoline N atom.

4-Nitro-N-(8-quinol­yl)benzene­sulfonami
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In the title compound, C 15 H 11 N 3 O 4 S, the dihedral angle between the quinoline ring system and the benzene ring is 79.9 (3) . Intermolecular hydrogen bonds of types N-HÁ Á ÁO, C-HÁ Á ÁO and C-HÁ Á ÁN are observed.

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In the crystal structure of the title compound, C 26 H 34 N 2 O 3 S, the quinoline ring system, with methoxy and methyl substituents, is nearly planar. An intramolecular hydrogen bond [N-HÁ Á ÁN = 2.16 (2) A ˚] is observed.

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In the title compound, C 13 H 12 F 3 N 5 O 2 , intramolecular N-HÁ Á ÁF, N-HÁ Á ÁN, C-HÁ Á ÁO and C-HÁ Á ÁN hydrogen bonds, andstacking interactions generate a columnar structure along the a axis.