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N-(3-Nitro­phen­yl)-1-oxo-2,6,7-trioxa-1-phosphabicyclo­[2.2.2]octane-4-carboxamide dimethyl­formamide solvate

✍ Scribed by Zang, Hong-Jun ;Guo, Ming-Lin ;Cheng, Bo-Wen ;Ren, Yuan-Lin

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
294 KB
Volume
61
Category
Article
ISSN
1600-5368

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✍ Zang, Hong-Jun ;Guo, Ming-Lin 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 352 KB

In the title compound, C 11 H 11 N 2 O 7 P, compression of the P-O-C angles is observed, suggesting that some strain is probably present. The configuration around phosphorus is distorted tetrahedral. In the crystal structure, N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen-bond contacts and van der Waals forces st

N-[2-(Amino­carbon­yl)phen­yl]-4-hydr­ox
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In the title compound, C 17 H 15 N 3 O 5 SÁC 2 H 6 OS, the thiazine ring adopts a distorted half-chair conformation. The enolic H atom is involved in both intramolecular and intermolecular O-HÁ Á ÁO hydrogen bonds, the latter linking the molecules into centrosymmetric pairs. Both anthranilamide H at