N-[3-(2-Nitrophenyl)allylidene]naphthalen-1-amine
✍ Scribed by Yang, Xiao-Yan ;He, Xiao-Lian ;Li, Ying ;Bi, Sai
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 434 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
In the crystal structure of the title compound, C 19 H 14 N 2 O 2 , the molecules are almost planar. The dihedral angle between the two aromatic ring systems is 3.67 (1) .
Related literature
For related literature, see: Yang et al. (2006). Experimental Crystal data C 19 H 14 N 2 O 2 M r = 302.32 Monoclinic, P2 1 =c a = 15.440 (2) A ˚b = 7.4165 (10) A c = 14.598 (2) A = 117.347 (2) V = 1484.7 (3) A ˚3 Z = 4 Mo K radiation = 0.09 mm À1 T = 293 (2) K 0.42 Â 0.26 Â 0.05 mm Data collection Siemens SMART 1000 CCD areadetector diffractometer Absorption correction: multi-scan (SADABS; Sheldrick, 1996) T min = 0.964, T max = 0.996 8073 measured reflections 2913 independent reflections 2014 reflections with I > 2(I) R int = 0.039 Refinement R[F 2 > 2(F 2 )] = 0.047 wR(F 2
📜 SIMILAR VOLUMES
In the title compound, C~21~H~18~N~2~·CH~4~O, the two naphthyl ring systems are arranged almost orthogonal to one another, with a dihedral angle of 89.8 (1)°.
Powder X-ray study T = 295 K Mean '(C±C) = 0.006 A Ê R factor = 0.045 wR factor = 0.060 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.