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Multiple Electrophilic Substitution of 1,1,2,2,9,9,10,10-Octafluoro[2.2]paracyclophane

✍ Scribed by Roche, Alex J.; Dolbier, William R.

Book ID
127232385
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
114 KB
Volume
65
Category
Article
ISSN
0022-3263

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Full multinuclear resonance analysis of
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The complete assignment of 19 F, 1 H and 13 C NMR spectra for a monosubstituted octafluoro[2.2]paracyclophane derivative is described for the first time. The unambiguous assignments were achieved through the combination of 19 F-1 H HOESY, 1 H COSY and 19 F COSY techniques and then further confirmed

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## Abstract The radical anion of 1,1,2.2,9,9,10, 10‐octafluoro[2.2]paracyclophane (**1**) has been generated by electrolytic reduction of **1** in 1,2‐dimethoxyethane (tetrabutylammonium perchlorate as the supporting salt). The hyperfine coupling constants of the eight ^19^F‐nuclei and the eight pr