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ChemInform Abstract: Novel Ring-Cleaving Reaction of 4-Nitro-1,1,2,2,9,9,10,10-octafluoro[2.2]paracyclophane with Nucleophiles.

✍ Scribed by William R. Jr. Dolbier; Yian Zhai; Wei Xu; Will Wheelus; Florian Dulong; Efram Goldberg; Ion Ghiviriga; Merle A. Battiste

Publisher: John Wiley and Sons
Year: 2009
Weight: 23 KB
Volume: 40
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200916034

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## Abstract The title compounds 8 and 1 have been synthesized in three steps each from 1,2‐dibromo[2.2]paracyclophan‐1‐ene (2) and 1,2,9,10‐tetrabromo[2.2]paracyclophane‐1,9‐diene (4), respectively. Copper‐mediated coupling of vinyl bromides 2 and 4 with methyl‐ and phenylmagnesium bromide gives su

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