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A Novel, Non-High-Dilution Method for Preparation of 1,1,2,2,9,9,10,10-Octafluoro[2.2]paracyclophane

✍ Scribed by Dolbier,, William R.; Duan, Jian-Xin; Roche, Alex J.


Book ID
126973858
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
109 KB
Volume
2
Category
Article
ISSN
1523-7060

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## Abstract The radical anion of 1,1,2.2,9,9,10, 10‐octafluoro[2.2]paracyclophane (**1**) has been generated by electrolytic reduction of **1** in 1,2‐dimethoxyethane (tetrabutylammonium perchlorate as the supporting salt). The hyperfine coupling constants of the eight ^19^F‐nuclei and the eight pr