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Multi-Step Synthesis by Using Modular Flow Reactors: The Preparation of YneOnes and Their Use in Heterocycle Synthesis

✍ Scribed by Ian R. Baxendale; Søren C. Schou; Jörg Sedelmeier; Steven V. Ley

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
650 KB
Volume
16
Category
Article
ISSN
0947-6539

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Multistep Synthesis Using Modular Flow R
Multistep Synthesis Using Modular Flow Reactors: Bestmann–Ohira Reagent for the Formation of Alkynes and Triazoles
✍ Ian R. Baxendale; Steven V. Ley; Andrew C. Mansfield; Christopher D. Smith 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 546 KB

## Abstract **Multistep in flow:** The Seyferth–Gilbert reagent **1** has been applied in a flow system to rapidly synthesize terminal alkynes. The system has been further applied to synthesize triazole **3** from alcohol **2** in a three‐step oxidation/homologation/copper(I)‐catalyzed azide–alkyne