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Modern Magnetic Resonance || 1H and 13C High-Resolution Solid-State NMR of Paramagnetic Compounds Under Very Fast Magic Angle Spinning
โ Scribed by Webb, Graham A.
- Book ID
- 120161952
- Publisher
- Springer Netherlands
- Year
- 2006
- Weight
- 503 KB
- Category
- Article
- ISBN
- 1402039107
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๐ SIMILAR VOLUMES
The use of a low-power two-pulse phase modulation (TPPM) sequence is proposed for efficient 1 H radio frequency (rf) decoupling in high-resolution 13 C solid-state NMR (SSNMR) under fast MAS conditions. Decoupling efficiency for different low-power decoupling sequences such as continuous-wave (cw),
## Abstract We show how highโresolution magic angleโspinning NMR spectroscopy can be used to characterize ^13^Cโlabeled saccharides that have been prepared using solidโphase synthesis techniques while they are still bound to a solidโsupport resin. With the use of ^13^Cโlabeled glucose as the starti