ChemInform Abstract: 1H and 13C High-Resolution Solid-State NMR of Paramagnetic Compounds under Very Fast Magic Angle Spinning
✍ Scribed by Yoshitaka Ishii; Nalinda P. Wickramasinghe
- Publisher
- John Wiley and Sons
- Year
- 2008
- Weight
- 18 KB
- Volume
- 39
- Category
- Article
- ISSN
- 0931-7597
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✦ Synopsis
Abstract
ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable via the “References” option.
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## Abstract We show how high‐resolution magic angle‐spinning NMR spectroscopy can be used to characterize ^13^C‐labeled saccharides that have been prepared using solid‐phase synthesis techniques while they are still bound to a solid‐support resin. With the use of ^13^C‐labeled glucose as the starti
## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable v
The assignment of nonexchanging protons of a small microcrystalline protein, the alpha-spectrin SH3 domain (7.2 kDa, 62 residues), was achieved by means of three-dimensional (3D) heteronuclear (1H-13C-13C) magic-angle spinning (MAS) NMR dipolar correlation spectroscopy. With the favorable combinatio