Microwave-induced One-pot Synthesis of N-carboxyalkyl Maleimides and Phthalimides†
✍ Scribed by Borah, Harsha N.; Boruah, Romesh C.; Sandhu, Jagir S.
- Book ID
- 121507738
- Publisher
- Science Reviews 2000 Ltd
- Year
- 1998
- Tongue
- English
- Weight
- 98 KB
- Volume
- 5
- Category
- Article
- ISSN
- 0308-2342
- DOI
- 10.1039/A707961C
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📜 SIMILAR VOLUMES
A novel and efficient microwave-assisted one-step reaction was developed to synthesize chiral N-sulfonylaziridines by the reaction of different chiral amino alcohols and sulfonic chlorides. The newly developed microwave synthetic method has the advantage of reducing the reaction time from 24 to 0.5
Substituted phthalimides and naphthalmlides have been obtained in good to excellent yields, employing chlorotrimethylsilane and sodium iodide (in sit. generation of iodotrimethylsilane) from corresponding azidcs and anhydrides under mild conditions.