𝔖 Bobbio Scriptorium
✦   LIBER   ✦

One-pot and microwave-assisted synthesis of N-sulfonylaziridines

✍ Scribed by Hao Xu; Hua Tian; Liangyu Zheng; Qingwen Liu; Li Wang; Suoqin Zhang

Book ID
104099107
Publisher
Elsevier Science
Year
2011
Tongue
French
Weight
339 KB
Volume
52
Category
Article
ISSN
0040-4039

No coin nor oath required. For personal study only.

✦ Synopsis

A novel and efficient microwave-assisted one-step reaction was developed to synthesize chiral N-sulfonylaziridines by the reaction of different chiral amino alcohols and sulfonic chlorides. The newly developed microwave synthetic method has the advantage of reducing the reaction time from 24 to 0.5 h with improved yields (84-93%) and minimizing by-products.

📜 SIMILAR VOLUMES

Microwave-Assisted One-Pot Synthesis of
Microwave-Assisted One-Pot Synthesis of 1,2,3,4-Tetrahydrocarbazoles.
✍ Jing Chen; Yongzhou Hu 📂 Article 📅 2006 🏛 John Wiley and Sons ⚖ 17 KB 👁 1 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract, please click on HTML or PDF.

One-pot-one-step, microwave-assisted Fis
One-pot-one-step, microwave-assisted Fischer indole synthesis
✍ Evelyn Cuevas Creencia; Masayuki Tsukamoto; Takaaki Horaguchi 📂 Article 📅 2011 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 174 KB

## Abstract The Fischer indole synthesis was carried out using microwaves instead of conventional heating procedures. When the mixture of phenylhydrazine, cyclohexanone and zinc chloride was irradiated at 600 W for 3 min, 76% of 1,2,3,4‐tetrahydrocarbazole was obtained. However, when zinc chloride