In the molecule of the title compound, C 15 H 13 ClN 2 O 4 , the pyrimidine and benzene rings form a dihedral angle of 69.3 (3) . Nostacking interactions are observed in the crystal structure.
Methyl 2-(4-methoxypyrimidin-2-ylcarbamoylsulfamoyl)benzoate
✍ Scribed by Ma, Ning ;Wang, Baolei ;Wang, Jianguo ;Song, Haibin ;Wang, Suhua ;Li, Zhengming
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 249 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.056 wR factor = 0.119 Data-to-parameter ratio = 14.9
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The title compound, C 27 H 24 ClN 3 O 6 , a probable new herbicide, was synthesized by the reaction of 4,6-dimethoxy-2-(methylsulfonyl)pyrimidine and methyl 4-[2-chloro-4-(2-hydroxybenzylamino)phenoxy]benzoate in tetrahydrofuran. -Interactions occur between neighbouring benzene rings.
The title compound, C~26~H~26~N~2~O~7~, is a thiamidine derivative. Geometric parameters are in the usual ranges. The crystal packing is stabilized by a classical N—H...O hydrogen bond, several weak C—H...O hydrogen bonds and a π–π stacking interaction.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.045 wR factor = 0.125 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 15 H 14 O 2 , the dihedral angle between the two benzene rings is 56.34 (7) .