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(E)-Methyl 2-[2-(6-chloropyrimidin-4-yloxy)phenyl]-3-methoxyacrylate

✍ Scribed by Ma, Hong-Fei ;Jia, Hong-Sheng ;Liu, Shan ;Wen, Fan ;Chen, Bin-Lin

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 150 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536806055516

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✦ Synopsis

In the molecule of the title compound, C 15 H 13 ClN 2 O 4 , the pyrimidine and benzene rings form a dihedral angle of 69.3 (3) . Nostacking interactions are observed in the crystal structure.

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In the title compound, C 16 H 13 ClN 2 O 2 , the dihedral angle between the pyridine and benzene rings is 40.1 (1) . There is a weak intramolecular C-HÁ Á ÁCl interaction. Molecules are linked via O-HÁ Á ÁN hydrogen bonds, forming chains of graph-set motif C(6) along the a axis.

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✍ Khanum, S. A. ;Mahendra, M. ;Shashikanth, S. ;Doreswamy, B. H. ;Sridhar, M. A. ; 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 246 KB

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In the title compound, C 19 H 18 NO 2 + . C 7 H 7 SO 3 À , the cation is almost planar and the benzene ring of the anion makes dihedral angles of 59.17 (9) and 60.59 (10) with the mean planes through the quinolinium and benzene ring of the cation, respectively. The cations and anions are packed as a

(E)-Methyl 2-[2-(6-chloro­pyrimidin-4-yl­oxy)phen­yl]-3-methoxy­acrylate

✦ Synopsis

(E)-Methyl 2-[2-(6-chloropyrimidin-4-yloxy)phenyl]-3-methoxyacrylate