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Methods for the Cleavage of Allylic and Propargylic C—N Bonds in Amines and Amides — Selected Alternative Applications of the 1,3-Hydrogen Shift

✍ Scribed by Stephanie Escoubet; Stephane Gastaldi; Michele Bertrand

Publisher: John Wiley and Sons
Year: 2005
Weight: 8 KB
Volume: 36
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200550249

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✦ Synopsis

Abstract

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## Abstract An operationally simple and highly efficient methodology for the removal of the allyl protecting group in amides and lactams has been developed by using the commercially available bis(allyl)–ruthenium(IV) catalysts [Ru(η^3^:η^2^:η^3^‐C~12~H~18~)Cl~2~] (C~12~H~18~=dodeca‐2,6,10‐triene‐1,