The title compound, C 6 H 12 O 6 , has been obtained from the ethanol fraction of the aerial part of the plant Incarvillea emodi (Wall. ex Royle) Chatterjee, after recrystallization from ethanol/ethyl acetate (60:40). Each molecule is involved in 12 hydrogen bonds, as has been found in other reporte
Malonamide: an orthorhombic polymorph
✍ Scribed by Nichol, Gary S. ;Clegg, William
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 237 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
An orthorhombic polymorph of malonamide, C 3 H 6 N 2 O 2 , is reported. The unit-cell dimensions, crystallographic symmetry and some aspects of the molecular geometry are significantly different from those of the known monoclinic form [Chieh et al. (1970). J. Chem. Soc. A, pp. 179-184] and of the tetragonal form described in the previous paper [Nichol & Clegg (2005). Acta Cryst. E61, o3424-o3426]. A simple R 4
📜 SIMILAR VOLUMES
A new polymorph of the title compound {systematic name: 2-[(__S__)-1-azoniabicyclo[2.2.2]oct-3-yl]-2,3,3a,4,5,6-hexahydro-1__H__-benz[__de__]isoquinolin-1-one chloride}, C~19~H~25~ON~2~ ^+^·Cl^−^, an anti-emetic and antinausea agent, has been obtained by crystallization from dimethylformamide. In th