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Liquid chromatographic determination of alkylthiols via derivatization with 5,5'-dithiobis(2-nitrobenzoic acid)

โœ Scribed by Kuwata, Kazuhiro.; Uebori, Michiko.; Yamada, Kazuhiko.; Yamazaki, Yoshiaki.


Book ID
126453794
Publisher
American Chemical Society
Year
1982
Tongue
English
Weight
731 KB
Volume
54
Category
Article
ISSN
0003-2700

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Determination of hydrogen sulfide with 5
โœ Aws S. Nashef; David T. Osuga; Robert E. Feeney ๐Ÿ“‚ Article ๐Ÿ“… 1977 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 660 KB

Hydrogen sulfide was determined with N-ethylmaleimide (NEM), p-chloromercuribenzoate (PCMB), and 5,5'-dithiobiQ2nitrobenzoic acid) (DTNB). One mole of hydrogen sulfide reacted with two moles of NEM or PCMB. It reacted with only one mole of DTNB, but produced two moles of the thiol anion, 5thio-2nitr