Ligand-Exchange Detection of Phosphorylated Peptides Using Liquid Chromatography Electrospray Mass Spectrometry
✍ Scribed by Krabbe, J. G.; Lingeman, H.; Niessen, W. M. A.; Irth, H.
- Book ID
- 127297579
- Publisher
- American Chemical Society
- Year
- 2003
- Tongue
- English
- Weight
- 190 KB
- Volume
- 75
- Category
- Article
- ISSN
- 0003-2700
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Linalool, nerol, geraniol, citronellol and a-terpineol were phosphorylated and the products purified by adsorption chromatography on XAD-2. High performance liquid chromatography-tandem mass spectrometry (LC-MSMS) analysis using the electrospray ionization technique (ESI) revealed the occurrence of
## Abstract Fused‐silica packed LC capillaries were interfaced with a triple quadrupole mass spectrometer through the electrospray ionization device. The coupling of these powerful techniques is suitable for structural characterization of constituents of peptide maps generated at high sensitivity.