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Lewis Acid Catalyst Free Electrophilic Alkylation of Silicon-Capped π Donors in 1,1,1,3,3,3-Hexafluoro-2-propanol

✍ Scribed by Maxim O. Ratnikov; Vasily V. Tumanov; William A. Smit

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
292 KB
Volume
47
Category
Article
ISSN
0044-8249

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ChemInform Abstract: Lewis Acid Catalyst
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Ring-Opening of 1-CF3-Substituted Epoxy
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Ring-opening of 1-CF 3 -substituted epoxy ethers with carboxylic acids was achieved in Et 3 N as solvent, and α-CF 3 -substituted acyloins and corresponding esters were obtained in good yields. In hexafluoro-2-propanol (HFIP) as solvent, the carboxylic acids acted as nucleophiles, and α-carbonyloxy