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Iodine mediated synthesis of alkyl tertio-alkyl ethers

✍ Scribed by G. Jenner


Book ID
104221313
Publisher
Elsevier Science
Year
1988
Tongue
French
Weight
182 KB
Volume
29
Category
Article
ISSN
0040-4039

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Tritium-or 14C-labelled methyl iodide and ethyl iodide were used for alkylations of phenols and thiols. The reactions were performed in a two-phase system with phase transfer catalysis at room temperature. Products of high specific activity were isolated in isotope yields ranging from 38% to 100%.