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Phase transfer mediated synthesis of radiolabelled alkyl aryl ethers and sulphides

✍ Scribed by Åke Bergman; Carl Axel Wachtmeister

Publisher
John Wiley and Sons
Year
1987
Tongue
French
Weight
258 KB
Volume
24
Category
Article
ISSN
0022-2135

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✦ Synopsis

Tritium-or 14C-labelled methyl iodide and ethyl iodide were used for alkylations of phenols and thiols. The reactions were performed in a two-phase system with phase transfer catalysis at room temperature. Products of high specific activity were isolated in isotope yields ranging from 38% to 100%.

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