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In-situ deactivation of packed columns for SFC

✍ Scribed by Zhang, Shigang ;Schindler, Brigitte ;Nicholson, Graham ;Bayer, Ernst

Publisher
John Wiley and Sons
Year
1995
Tongue
English
Weight
237 KB
Volume
18
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

Residual adsorptive activity of reversed phase (RP) column packings used in supercritical fluid chromatography (SFC) can be significantly reduced by a dynamic in‐situ silanization with diphenyltetramethyldisilazane (DPTMDS). RP‐materials thus deactivated were characterized both chromatographically and by solid‐phase ^29^Si NMR.

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