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Improved synthesis of deuterated olefins from the Wittig reaction

โœ Scribed by Buchanan, Gerald W.; Gustafson, Albert E.

Book ID
126414511
Publisher
American Chemical Society
Year
1973
Tongue
English
Weight
303 KB
Volume
38
Category
Article
ISSN
0022-3263

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Thp Wittig synthesis has been used to prepare conveniently carbon-14 labeled 1-olejh in the Cs to c 8 range in about 60 % yield. Thp chemicd and radiochemical purities of the products exceeded 99.5 %, The common source of carbon-14 in these reactions was methyl-14C-triphenylphosphonium iodide which