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Deuterated Olefins from the Wittig Reaction

โœ Scribed by Malloy, Jr., Thomas; Hedges, Richard; Fisher, Farley


Book ID
127136462
Publisher
American Chemical Society
Year
1970
Tongue
English
Weight
331 KB
Volume
35
Category
Article
ISSN
0022-3263

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cis -OLEFINS FROM THE WITTIG REACTION
โœ Sonnet, P. E. ๐Ÿ“‚ Article ๐Ÿ“… 1974 ๐Ÿ› Taylor and Francis Group ๐ŸŒ English โš– 166 KB
Synthesis of 14C-labeled olefins using t
โœ M. A. Muhs ๐Ÿ“‚ Article ๐Ÿ“… 1968 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 412 KB

Thp Wittig synthesis has been used to prepare conveniently carbon-14 labeled 1-olejh in the Cs to c 8 range in about 60 % yield. Thp chemicd and radiochemical purities of the products exceeded 99.5 %, The common source of carbon-14 in these reactions was methyl-14C-triphenylphosphonium iodide which