Improved methods for thin-layer chromatographic separation of 2,4-dinitrophenylhydrazones
โ Scribed by Aage Jart; Allan J. Bigler
- Publisher
- Elsevier Science
- Year
- 1966
- Tongue
- English
- Weight
- 543 KB
- Volume
- 23
- Category
- Article
- ISSN
- 1873-3778
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๐ SIMILAR VOLUMES
For characterizing keto acids, paper chromatography of their DNPHa is most widely used irrespective of the disadvantages (1)) some of which are as follows: According to the methods reported before 1962, the DNPH formed by the usual method were extracted from water solution with an organic solvent su
Thin-layer chromatography of keto acid 2,4-dinitrophenylhydrazones was carried out on plate coated with silica gel and sodium bicarbonate. A clear separation was obtained between most of the various keto acid hydrazones. The hydrazone was eluted from the plate with methanol containing 1% concentrate