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Improved etherification procedure for the preparation of dibenz[b,f][1,4]oxazepine

✍ Scribed by H. Fakhraian; Y. Nafary; A. Yarahmadi; H. Hadj-Ghanbary

Publisher
Journal of Heterocyclic Chemistry
Year
2008
Tongue
English
Weight
200 KB
Volume
45
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

magnified image

The effect of temperature and catalyst on the yield and rate of the etherification reaction between 1 and 2 was investigated and alternative methods for separation of 3 and 4 from the reaction mixture have been described.

πŸ“œ SIMILAR VOLUMES

ChemInform Abstract: Improved Etherifica
ChemInform Abstract: Improved Etherification Procedure for the Preparation of Dibenz[b,f][1,4]oxazepine.
✍ H. Fakhraian; Y. Nafary; A. Yarahmadi; H. Hadj-Ghanbary πŸ“‚ Article πŸ“… 2009 πŸ› John Wiley and Sons βš– 26 KB πŸ‘ 2 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 200 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a β€œFull Text” option. The original article is trackable v

Reinvestigation of alternative method fo
Reinvestigation of alternative method for the preparation of dibenz[b,f][1,4]oxazepine
✍ Hossein Fakhraian; Yaser Nafary πŸ“‚ Article πŸ“… 2009 πŸ› Journal of Heterocyclic Chemistry 🌐 English βš– 86 KB πŸ‘ 1 views

## Abstract magnified image Two distinct alternative methods using different starting materials for the preparation of dibenz[__b__,__f__][1, 4]oxazepine (**7**, CR) were reinvestigated. The possibility of __trans‐cis__ conversion of the Schiff base **5cis**, **5trans** (produced from **1** and **

The synthesis and chemistry of [11-14C]-
The synthesis and chemistry of [11-14C]-dibenz[b,f] [1,4]oxazepine
✍ J. M. Harrison; T. D. Inch; D. G. Upshall πŸ“‚ Article πŸ“… 1978 πŸ› John Wiley and Sons 🌐 French βš– 211 KB

## Abstract The synthesis of [11‐^14^C]‐dibenz[b,f][1,4]oxazepine 1 is described. Chromium trioxide – pyridine oxidation of 1 gives [11‐^14^C]‐10, 11‐dihydrodibenz [b,f][1,4] oxazepin‐11‐one 3 which on hydrolysis gives 2‐amino‐2′‐[^14^C]‐carboxydiphenylether 4. Hydrogenation of 1 affords [11‐^14^C]