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Improved cross-axis synchronous flow-through coil planet centrifuge for performing counter-current chromatography : I. Design of the apparatus and analysis of accelaration

โœ Scribed by Yoichiro Ito; Hisao Oka; Jimmie L. Slemp


Publisher
Elsevier Science
Year
1989
Tongue
English
Weight
784 KB
Volume
463
Category
Article
ISSN
1873-3778

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โœฆ Synopsis


A novel design of the cross-axis synchronous flow-through coil planet centrifuge is introduced. The apparatus holds a pair of large coil holders symmetrically, one on each side of the rotary frame, at a lateral position 12.5 cm from the center of the holder shaft held 10 cm from the centrifuge axis. Mathematical analysis of acceleration generated by the planetary motion of the apparatus revealed a unique centrifugal force field which promises high retention of the stationary phase in the multilayer coil to perform efficient preparative-scale counter-current chromatography.


๐Ÿ“œ SIMILAR VOLUMES


Improved cross-axis synchronous flow-thr
โœ Molina Bhatnagar; Hisao Oka; Yoichiro Ito ๐Ÿ“‚ Article ๐Ÿ“… 1989 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 977 KB

Performance of the apparatus was evaluated in terms of stationary phase retention, partition efficiency and sample loading capacity. Preliminary studies with short coils revealed high retention of the stationary phase under a proper combination of the head-tail elution and planetary motion. Preparat

Cross-axis synchronous flow-through coil
โœ Yoichiro Ito; Tian-you Zhang ๐Ÿ“‚ Article ๐Ÿ“… 1988 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 501 KB

A series of experiments was conducted to evaluate the partition efficiency of the cross-axis synchronous flow-through coil planet centrifuge. The preliminary studies indicated that short coils (5 m) mounted on 15-and 25-cm diameter holders in either a central or a lateral location produce a high par