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Highly Diastereoselective Ketone Aldol Reactions of Butane-2,3-diacetal Desymmetrized Glycolic Acid.

✍ Scribed by Darren J. Dixon; Antonio Guarna; Steven V. Ley; Alessandra Polara; Felix Rodriguez

Publisher: John Wiley and Sons
Year: 2003
Weight: 160 KB
Volume: 34
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200306089

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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37 8C) and the mixture was filtered in a UltraFree MC 30 000 MWCO centrifugal filtration unit (Millipore) at 3500 g for 7 min at 37 8C. The concentration of free substrate in the filtrate was quantified by ICP-MS and the bound fraction was calculated as % bound ([total]-[free])/[total]. The proton T