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High Throughput Synthesis of Peptide α-Thioesters Through the Use of “Volatilizable” Support

✍ Scribed by Li, Yangmei; Yu, Yongping; Giulianotti, Marc; Houghten, Richard A.

Book ID
120027027
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
294 KB
Volume
10
Category
Article
ISSN
1520-4766

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A facile approach to the synthesis of 3,4-disubstituted-2-aminothiazolium derivatives through the use of a ‘volatilizable’ support
✍ Yangmei Li; Marc Giulianotti; Richard A. Houghten 📂 Article 📅 2010 🏛 Elsevier Science 🌐 French ⚖ 190 KB

A facile solid-phase synthetic approach to the synthesis of 3,4-disubstituted-2-aminothiazolium derivatives was reported. Functionalized aminomethylphenyl silica gel was used as a 'volatilizable' support. The products were cleaved with 10% HF and were obtained in high yields and purities.