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High-throughput assay of rotenone in olive oil using atmospheric pressure chemical ionization tandem mass spectrometry

✍ Scribed by Leonardo di Donna; Giovanni Grassi; Fabio Mazzotti; Enzo Perri; Giovanni Sindona

Publisher
John Wiley and Sons
Year
2004
Tongue
English
Weight
100 KB
Volume
39
Category
Article
ISSN
1076-5174

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✦ Synopsis

Abstract

A high‐throughput method is presented for the determination of rotenone in contaminated matrices. The procedure involves atmospheric pressure chemical ionization tandem mass spectrometry with a triple‐quadrupole instrument and the use as internal standard of a cycloadduct derivative of rotenone itself. The method was applied to the evaluation of the decay of rotenone in olives and olive oil at various times after exposure to the contaminant. Copyright © 2004 John Wiley & Sons, Ltd.

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